참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2,4-Dinitrophenol | HCID 1493 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 2-Butene, 1,4-dibromo- | HCID 13180 | — |
| 용매 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 생성물 | 1-Bromo-4-(2,4-dinitrophenyloxy)but-2-ene | HCID 73994034 | 46.7% |
반응 단계
A mixture of 2,4-dinitrophenol (4.6 g, 80 wt %), potassium carbonate (4.2 g), NMP (40 mL) and 1,4-dibromo-2-butene (12.8 g) was heated to 45° C. for 2 hr. Extraction in the normal fashion and Kugelrohr distillation of the excess dibromide (0.1 mm Hg, 80° C.) gave 1-bromo-4-(2,4-dinitrophenyloxy)but-2-ene (3.7 g, mp 55-57° C.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06713135B2 |
|---|
| 출처 데이터셋 | uspto-grants-2004_03 |
|---|
| ORD ID | ord-001383a7dc4048e8b945bdebc5387987 |
|---|
| 출처 메모 | uspto-grants-2004_03 |
|---|
