4-((Trifluoromethyl)thio)aniline → 2-[4-(dimethylamino)phenyl]-N-{4-[(trifluoromethyl)thio]phenyl}acetamide

참여 물질

역할	이름	HCID	투입량
반응물	4-((Trifluoromethyl)thio)aniline	HCID 123054	—
반응물	4-N,N-dimethylaminophenylacetic acid	HCID 152203	—
생성물	2-[4-(dimethylamino)phenyl]-N-{4-[(trifluoromethyl)thio]phenyl}acetamide	HCID 44243115	—

반응 단계

The product was prepared from 2-(4-(dimethylamino)phenyl)acetic acid (23 mg) and 4-trifluoromethylthioaniline (28 mg) according to Method C: 1H NMR (300 MHz, CDCl3) δ ppm 2.98 (s, 6 H), 3.66 (s, 2 H), 6.72-6.78 (m, 2 H), 7.14-7.19 (m, 2 H), 7.19 (s, 1 H), 7.43-7.51 (m, 2 H), 7.52-7.57 (m, 2 H); MS (ESI-pos) m/z 355.0 (M+H)+.

출처 및 근거

DOI	10.6084/m9.figshare.5104873.v1
특허 번호	US07786171B2
출처 데이터셋	uspto-grants-2010_08
ORD ID	ord-f7b001fe97a5435f810370dd53f80a26
출처 메모	uspto-grants-2010_08