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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 507521생성일: 2026년 10월 25일

N-(2-Aminoethyl)ethyleneurea → HCID 60204268, 화합물

https://huagongshe.com/reaction/507521

반응식

참여 물질

역할이름HCID투입량
반응물N-(2-Aminoethyl)ethyleneureaHCID 80480—
반응물HCID 15141655HCID 15141655—
용매IsopropanolHCID 3776—
생성물HCID 60204268HCID 6020426868%

반응 단계

A mixture of 4-(5-bromothiophen-2-yl)-2-chloropyrimidine (1.0 g, 3.63 mmol), 1-(2-aminoethyl)imidazolidin-2-one (0.47 g, 3.63 mmol) and triethylame (0.44 g, 4.36 mmol) in isopropanol (25 mL) was refluxed for 30 h. After cooling down to rt the precipitate was filtered and washed with methanol (5 mL) and dried to give the title compound as a yellow solid (0.9 g, 68%). MS (M+H)+ 368/370.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07786132B2
출처 데이터셋uspto-grants-2010_08
ORD IDord-177cb6d9dcaf40178917a7289810f389
출처 메모uspto-grants-2010_08