Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → (2r)-3-Aza-2-phenyl-4-(3,5-dimethylphenyl)but-3-en-1-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | Benzaldehyde, 3,5-dimethyl- | HCID 34225 | — |
| 반응물 | 2-Amino-2-phenylethanol | HCID 92466 | — |
| 생성물 | (2r)-3-Aza-2-phenyl-4-(3,5-dimethylphenyl)but-3-en-1-ol | HCID 68464252 | — |
반응 단계
A solution of 3,5-dimethylbenzaldehyde (30.0 g) and (R)-phenylglycinol (30.7 g) in toluene (200 ml) was refluxed for 3 hours with removing water. The reaction solution was concentrated to give the title compound (59.7 g) having the following physical data.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07786161B2 |
| 출처 데이터셋 | uspto-grants-2010_08 |
| ORD ID | ord-4f181c044fb94d2fad5acf4989f8d97a |
| 출처 메모 | uspto-grants-2010_08 |