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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 50875생성일: 2026년 10월 27일

2,6-Dichloropyridine → (E)-1-(6-chloropyridin-2-yl)-2-styryl-1H-benzimidazole

https://huagongshe.com/reaction/50875

반응식

참여 물질

역할이름HCID투입량
반응물2,6-DichloropyridineHCID 16989—
반응물2-(2-Phenylethenyl)-1h-benzimidazoleHCID 242965—
반응물(E)-1-(2-pyridyl)-2-styryl-1H-benzimidazoleHCID 9796241—
생성물(E)-1-(6-chloropyridin-2-yl)-2-styryl-1H-benzimidazoleHCID 22736737—

반응 단계

Free base of the titled compound was prepared from 2-styryl-1H-benzimidazole and 2,6-dichloropyridine according to the preparation of (E)-1-(2-pyridyl)-2-styryl-1H-benzimidazole (Example 1, method B). MW: 331.81; mp: 122.0-123.0° C.; 1H-NMR (DMSO) δ: 8.22 (1H, t, J=7.9 Hz), 7.91 (1H, d, J=16.1 Hz), 7.79-7.72 (3H, m), 7.67-7.63 (2H, m), 7.50-7.47 (1H, m), 746-7.28 (5H, m), 7.23 (1H, d, J=16.1 Hz).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06713482B2
출처 데이터셋uspto-grants-2004_03
ORD IDord-816abe7237094fe3ac23eee9419270c4
출처 메모uspto-grants-2004_03