Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → Methyl 3-thienylacetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 3-Thiophenacetic acid | HCID 23404 | — |
| 생성물 | Methyl 3-thienylacetate | HCID 94041 | — |
반응 단계
To 2-(thiophen-3-yl)acetic acid in MeOH at 0° C. was added TMS-CH2N2. The solution was stirred for 3 hours then quenched with a few drops of AcOH. The solvents were evaporated. Column chromatography (SiO2, 3-15% EtOAc/Hex) gave pure methyl 2-(thiophen-3-yl)acetate (E41).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09096569B2 |
| 출처 데이터셋 | uspto-grants-2015_08 |
| ORD ID | ord-a19af21a912d4b2f89b4a2c300d895d3 |
| 출처 메모 | uspto-grants-2015_08 |