Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Benzylamino)-1-methylcyclohexanol → Trans-4-amino-1-methyl-cyclohexanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Benzylamino)-1-methylcyclohexanol | HCID 67465205 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Trans-4-amino-1-methyl-cyclohexanol | HCID 18331273 | 83% |
반응 단계
4-(Benzylamino)-1-methylcyclohexanol (335 mg, 1.53 mmol) was dissolved in EtOH (7.95 ml), followed by addition of Pd (10 wt % on activated carbon, 35 mg), and then the resulting liquid was stirred at room temperature under hydrogen stream for 31 hours. The resulting reaction liquid was filtered, concentrated under reduced pressure, and dried under vacuum, to obtain 164 mg of white solid (83%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09096571B2 |
| 출처 데이터셋 | uspto-grants-2015_08 |
| ORD ID | ord-791d899581944fa1a13752746fd44160 |
| 출처 메모 | uspto-grants-2015_08 |