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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 509292생성일: 2026년 10월 27일

4-(Benzylamino)-1-methylcyclohexanol → Trans-4-amino-1-methyl-cyclohexanol

https://huagongshe.com/reaction/509292

반응식

참여 물질

역할이름HCID투입량
반응물4-(Benzylamino)-1-methylcyclohexanolHCID 67465205—
촉매PalladiumHCID 23938—
용매EthanolHCID 702—
생성물Trans-4-amino-1-methyl-cyclohexanolHCID 1833127383%

반응 단계

4-(Benzylamino)-1-methylcyclohexanol (335 mg, 1.53 mmol) was dissolved in EtOH (7.95 ml), followed by addition of Pd (10 wt % on activated carbon, 35 mg), and then the resulting liquid was stirred at room temperature under hydrogen stream for 31 hours. The resulting reaction liquid was filtered, concentrated under reduced pressure, and dried under vacuum, to obtain 164 mg of white solid (83%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09096571B2
출처 데이터셋uspto-grants-2015_08
ORD IDord-791d899581944fa1a13752746fd44160
출처 메모uspto-grants-2015_08