Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cinnamoyl Chloride → (E)-6-Methyl-1-(2-pyridyl)-2-styryl-1H-benzimidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cinnamoyl Chloride | HCID 5354261 | — |
| 반응물 | (E)-1-(2-pyridyl)-2-styryl-1H-benzimidazole | HCID 9796241 | — |
| 반응물 | 2-amino-5-methyl-N-(2-pyridyl)aniline | HCID 22736708 | — |
| 생성물 | (E)-6-Methyl-1-(2-pyridyl)-2-styryl-1H-benzimidazole | HCID 22736763 | — |
반응 단계
The titled compound was prepared from 2-amino-5-methyl-N-(2-pyridyl)aniline and (E)-cinnamoyl chloride according to the preparation of (E)-1-(2-pyridyl)-2-styryl-1H-benzimidazole (Example 1, method A). MW: 311.39; mp: 164.0-164.9° C.; 1H-NMR (CDCl3) δ: 8.80-8.76 (1H, m), 8.03-7.92 (2H, m), 7.71 (1H, d, J=8.1 Hz), 7.54-7.42 (4H, m), 7.38-7.23 (4H, m), 7.19-7.14 (1H, m), 7.11 (1H, d, J=16.1 Hz), 2.46 (3H, s).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06713482B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-dedc25f6e8104377816b60455501a15a |
| 출처 메모 | uspto-grants-2004_03 |