Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanesulfonyl chloride → 3-Methoxybenzyl methanesulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanesulfonyl chloride | HCID 31297 | — |
| 반응물 | 3-Methoxybenzyl alcohol | HCID 81437 | — |
| 생성물 | 3-Methoxybenzyl methanesulfonate | HCID 15438579 | — |
반응 단계
The title compound was prepared by following the general procedure of Example 43 for mesylation as a colorless oil (292 mg, 93%) from 3-methoxybenzyl alcohol (200 mg, 1.45 mmol) and methanesulfonyl chloride (249 mg, 2.17 mmol). 1H NMR (CDCl3, 300 MHz) δ2.92 (s, 3H), 3.83 (s, 3H), 5.22 (s, 2H), 6.90-7.03 (m, 3H), 7.32 (t, 1H, J=7.7 Hz) ppm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06713471B1 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-4aae77ffae474e92b9425286f9f3309b |
| 출처 메모 | uspto-grants-2004_03 |