6-Chloro-2-phenyl-4H-3,1-benzoxazin-4-one → (2-Amino-5-chlorophenyl)(3-methoxyphenyl)methanone

HRID 513116

반응식

HRID 513116 반응식
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([Cl:8])=[CH:4][C:3]=1[C:9]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=1C)=[O:10].ClC1C=CC2N=[C:24](C3C=CC=CC=3)[O:25]C(=O)C=2C=1>>[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([Cl:8])=[CH:4][C:3]=1[C:9]([C:11]1[CH:16]=[CH:15][CH:14]=[C:13]([O:25][CH3:24])[CH:12]=1)=[O:10]

참가 물질

3

반응물 2

HCID 6910166-Chloro-2-phenyl-4H-3,1-benzoxazin-4-oneHCID 15592243(2-Amino-5-chlorophenyl)(2-methylphenyl)methanone

생성물 1

HCID 12325894(2-Amino-5-chlorophenyl)(3-methoxyphenyl)methanone수율 64%

실험 절차

In a manner similar to that described above for compound 1m, 6-chloro-2-phenyl-benzo[d][1,3]oxazin-4-one was converted to 1s (64% yield) MS m/z=262 (M+H).

출처 및 근거

ORD 기록
ord-ad74e0c6f5c44d5c9214e1ad699c229f
출처 데이터셋
uspto-grants-2015_08
특허 번호
US09102678B2

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