Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-butyl N-(4-chlorophenyl)carbamate → (2-Amino-5-chloro-phenyl)-(2,4-difluoro-phenyl)-methanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-butyl N-(4-chlorophenyl)carbamate | HCID 546372 | — |
| 반응물 | 2,4-Difluorobenzoyl chloride | HCID 588081 | — |
| 생성물 | (2-Amino-5-chloro-phenyl)-(2,4-difluoro-phenyl)-methanone | HCID 64423774 | 20% |
반응 단계
In a manner similar to that described above for compound 1aa, 4-Chloro-N-Boc-aniline and 2,4-difluoro-benzoyl chloride were converted to 1w (20% yield) MS m/z=268 (M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09102678B2 |
| 출처 데이터셋 | uspto-grants-2015_08 |
| ORD ID | ord-58cdec6ff740401b8563bb9cd855a2ab |
| 출처 메모 | uspto-grants-2015_08 |