Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Nitrobenzenesulfonyl chloride → N-(2-Methyl-quinolin-8-yl)-2-nitro-benzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Nitrobenzenesulfonyl chloride | HCID 15540 | — |
| 반응물 | 2-Methyl-8-aminoquinoline | HCID 140457 | — |
| 생성물 | N-(2-Methyl-quinolin-8-yl)-2-nitro-benzenesulfonamide | HCID 16759518 | 47% |
반응 단계
In a similar fashion using route 14 general procedure 26, 2-methyl-quinolin-8-ylamine (Intermediate 22) (417 mg, 2.64 mmol) and 2-nitrobenzensulfonyl chloride (643 mg, 2.64 mmol) gave the title compound (423 mg, 47%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09102688B2 |
| 출처 데이터셋 | uspto-grants-2015_08 |
| ORD ID | ord-c57e48eb75884d9cac5cdf631bac96a5 |
| 출처 메모 | uspto-grants-2015_08 |