Ethyl (2-chlorobenzoyl)acetate → HCID 178510209, 화합물

HRID 514331

반응식

HRID 514331 반응식
[NH:1]([C:3]1[CH:8]=[C:7]([C:9]#[N:10])[CH:6]=[CH:5][N:4]=1)[NH2:2].[Cl:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[C:18](=O)[CH2:19][C:20](OCC)=[O:21]>>[Cl:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[C:18]1[CH:19]=[C:20]([OH:21])[N:1]([C:3]2[CH:8]=[C:7]([C:9]#[N:10])[CH:6]=[CH:5][N:4]=2)[N:2]=1

참가 물질

3

반응물 2

HCID 292405Ethyl (2-chlorobenzoyl)acetateHCID 201187142-Hydrazinylpyridine-4-carbonitrile

생성물 1

HCID 178510209HCID 178510209, 화합물수율 75%

실험 절차

The title compound was prepared in 75% yield from 2-hydrazinylpyridine-4-carbonitrile (PREPARATION 2) and ethyl 3-(2-chlorophenyl)-3-oxopropanoate according to the procedure for the preparation of Example 3, part A. [M+H] Calc'd for C15H9ClN4O 297. Found, 297.

출처 및 근거

ORD 기록
ord-8a98c81085b84824880c5813279d7536
출처 데이터셋
uspto-grants-2015_08
특허 번호
US09107916B2

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