Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 2-Hydrazinylpyridine-4-carbonitrile hydrochloride salt
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 2-Hydrazinylpyridine-4-carbonitrile | HCID 20118714 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2-Hydrazinylpyridine-4-carbonitrile hydrochloride salt | HCID 86725484 | 95% |
반응 단계
To a solution of 2-hydrazinylpyridine-4-carbonitrile (2.13 g, 16 mmol, PREPARATION 2) in EtOAc (10 mL) was added HCl (4 M in EtOAc, 15 mL) at rt. It was then stirred at rt for 30 min. The reaction mixture was filtered and washed with EtOAc and dried to give the title compound (3.13 g, 95%) as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09107916B2 |
| 출처 데이터셋 | uspto-grants-2015_08 |
| ORD ID | ord-a78809a1a8e44a92b3a4ade8149e844e |
| 출처 메모 | uspto-grants-2015_08 |