Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Aminopyridine → N'-(2-Pyridyl)-N-methyl-N-phenylformamidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Aminopyridine | HCID 10439 | — |
| 반응물 | N-Methylformanilide | HCID 66737 | — |
| 생성물 | N'-(2-Pyridyl)-N-methyl-N-phenylformamidine | HCID 53887703 | — |
반응 단계
Prepared following the procedure of Example 1 from N-methylformanilide and 2-aminopyridine. Vacuum distillation of the crude product gave pure 3 as a pale yellow oil: bp 164°-165° C. @ 0.5 mm Hg. 1H-NMR (CDCl3) 8.94 (S, 1H), 8.30 (d, 1H, J=5 Hz), 7.6-6.9 (m,8H), 3.52 (S, 3H); IR(neat) 3045, 1620, 1580, 1555, 1500, 1460, 1435, 1235; MS (m/e) 211 (M+), 106 (base).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05243055 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-94e0b41df81646abb6a98f85deb9681f |
| 출처 메모 | uspto-grants-1993_09 |