Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Aminopyridine → N'-(2-Pyridyl)-N-ethyl-N-phenylformamidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Aminopyridine | HCID 10439 | — |
| 반응물 | Formamide, N-ethyl-N-phenyl- | HCID 79585 | — |
| 생성물 | N'-(2-Pyridyl)-N-ethyl-N-phenylformamidine | HCID 54151591 | — |
반응 단계
Prepared following the procedure of Example 1 from N-ethylformanilide and 2-aminopyridine. Vacuum distillation of the crude product gave pure 4 as a pale yellow oil: bp 164° C. @ 0.5 mm Hg. 1H-NMR (CDCl3) 8.83 (S, 1H), 8.30 (m,1H), 7.5-6.9 (m, 8H), 4.09 (q, 2H, J=7 Hz) 1.26 (t, 3H, J=7 Hz); IR(neat) 2990, 1620, 1570, 1500, 1460, 1440, 1390, 1230, 1130; MS (m/e) 225 (M+), 78 (base).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05243055 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-21c43fd9d87e46ca92b874799634794d |
| 출처 메모 | uspto-grants-1993_09 |