Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitric Acid → 2,9-Dimethyl-5-nitro-1,10-phenanthroline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 2,9-Dimethyl-1,10-phenanthroline | HCID 65237 | — |
| 생성물 | 2,9-Dimethyl-5-nitro-1,10-phenanthroline | HCID 379764 | — |
반응 단계
Specifically, 2,9-dimethyl-1,10-phenanthroline shown by the formula (A) in FIG. 1 is reacted with an acid mixture composed of nitric acid and sulfuric acid to give 5-nitro-2,9-dimethyl-1,10-phenanthroline shown by the formula (B) in FIG. 1. The 5-nitro-2,9-dimethyl-1,10-phenanthroline is then reacted with selenium dioxide to give a dialdehyde compound shown by the formula (C) in FIG. 1. This dialdehyde compound is then oxidized to obtain the compound of the formula (1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09110047B2 |
| 출처 데이터셋 | uspto-grants-2015_08 |
| ORD ID | ord-0f59cd525fb64804ac07fb173d4489ac |
| 출처 메모 | uspto-grants-2015_08 |