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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 516650생성일: 2026년 10월 23일

Methanol → HCID 178448544, 화합물

https://huagongshe.com/ko/reaction/516650

반응식

참여 물질

역할이름HCID투입량
반응물MethanolHCID 887—
반응물Potassium FluorideHCID 522689—
반응물1-Butyl-3-methylimidazolium chlorideHCID 2734161—
용매WaterHCID 962—
생성물HCID 178448544HCID 17844854494%

반응 조건

온도22 °C

반응 단계

10.3 grams of [BMIMCl] prepared as described above were added to a mixture of 28 mL methanol and 0.06 mL water. After complete dissolution of the [BMIMCl], 5.0 grams of dry potassium fluoride (KF) were added, and the reaction mixture was stirred at 22° C. for 20 minutes. The mixture was filtered. 4.4 grams of KF was added to the filtrate, and the mixing continued for additional 20 minutes. After filtration, the methanol was evaporated under vacuum at room temperature, and the mixture was then filtered and centrifuged. The resulting yellowish liquid was determined by elementary analysis to be the titled compound [BMIMF] in 94% yield.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09114360B2
출처 데이터셋uspto-grants-2015_08
ORD IDord-1ab9d796dbeb4188a89ff06eca4121c7
출처 메모uspto-grants-2015_08