참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methacrylic anhydride | HCID 12974 | — |
| 반응물 | 2-(N-ethylanilino)ethanol | HCID 62338 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 2-[Ethyl(phenyl)amino]ethyl prop-2-enoate | HCID 19097126 | — |
반응 단계
Methacrylic anhydride (7.7 g, 0.05 mol) is added to a solution of N-(2-hydroxyethyl)-N-ethylaniline (6.6 g, 0.04 mol) in pyridine (25 ml) and the mixture is stirred at 55° C. for 2 hours. On cooling the mixture is passed through silica gel to give N-(2-acryloyloxyethyl)-N-ethylaniline as a pale yellow oil. 5.3 g, 65%
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US09115464B2 |
|---|
| 출처 데이터셋 | uspto-grants-2015_08 |
|---|
| ORD ID | ord-b6a855aa18e948d3a1b8c85244d381bf |
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| 출처 메모 | uspto-grants-2015_08 |
|---|
