Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyrazole-4-carboxylic acid → N-{4-[4-(1-Pyrrolidinylmethyl)-2-pyridyloxy]-cis-2-butenyl}pyrazole-4-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyrazole-4-carboxylic acid | HCID 3015937 | — |
| 반응물 | 4-[4-(1-Pyrrolidinylmethyl)-2-pyridyloxy]-cis-2-butenylamine | HCID 15053128 | — |
| 생성물 | N-{4-[4-(1-Pyrrolidinylmethyl)-2-pyridyloxy]-cis-2-butenyl}pyrazole-4-carboxamide | HCID 67725971 | 34% |
반응 단계
Following a procedure similar to that described in Example 13, but using 4-[4-(1-pyrrolidinylmethyl)-2-pyridyloxy]-cis-2-butenylamine and 4-pyrazolecarboxylic acid as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained as a white powder, melting at 57°-61° C., in a 34% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05616579 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-65cbfa9f3d2f43d8a0423c90930c102f |
| 출처 메모 | uspto-grants-1997_04 |