Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-2-chloroacetamide → N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-2-(1-methyltetrazol-5-ylthio)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-2-chloroacetamide | HCID 67725626 | — |
| 반응물 | HCID 178482017 | HCID 178482017 | — |
| 생성물 | N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-2-(1-methyltetrazol-5-ylthio)acetamide | HCID 67726009 | 87% |
반응 단계
Following a procedure similar to that described in Example 33, but using N-[4-(4-piperidinomethyl-2-pyridyloxy) -cis-2-butenyl]-2-chloroacetamide (prepared as described in Preparation 1) and 1-methyl-5-mercaptotetrazole as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained as a white powder, melting at 58°-62° C., in an 87% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05616579 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-c0ab4787aa49412dbf05c8a6090b1db9 |
| 출처 메모 | uspto-grants-1997_04 |