2-Indanone → Azafluorene

HRID 521009노트

반응식

HRID 521009 반응식
[CH2:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH2:3][C:2]1=O.[CH2:11]([NH2:14])[C:12]#[CH:13]>>[N:14]1[CH:11]=[CH:12][CH:13]=[C:1]2[C:9]3[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=3[CH2:3][C:2]=12

참가 물질

3

반응물 2

HCID 119832-IndanoneHCID 239041Propargylamine

생성물 1

HCID 12226515Azafluorene수율 56%

실험 절차

The title compound is prepared from 2-indanone and propargylamine following a procedure analogous to that described in Step 1 of Intermediates 1 and 2. Yield: 56% of theory; Mass spectrum (ESI+): m/z=168 [M+H]+.

출처 및 근거

ORD 기록
ord-9442273d689a401ba57d532b4de0926c
출처 데이터셋
uspto-grants-2016_05
특허 번호
US09328072B2

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