Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,3-Dimethylbutanoyl chloride → N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-2-[2-(3,3-dimethylbutyryloxy)ethylthio)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,3-Dimethylbutanoyl chloride | HCID 81514 | — |
| 반응물 | N-[4-(4-piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-2-(2-hydroxyethylthio)acetamide | HCID 67725880 | — |
| 생성물 | N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-2-[2-(3,3-dimethylbutyryloxy)ethylthio)acetamide | HCID 67726203 | 83% |
반응 단계
Following a procedure similar to that described in Example 7, but using N-[4-(4-piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-2-(2-hydroxyethylthio)acetamide (prepared as described in Example 1) and 3,3-dimethylbutyryl chloride as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained in an 83% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05616579 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-268bfa98db9942d5bbe082505c234cb1 |
| 출처 메모 | uspto-grants-1997_04 |