Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Butyryl chloride → N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-2-(2-butyryloxyethylthio)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Butyryl chloride | HCID 8855 | — |
| 반응물 | N-[4-(4-piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-2-(2-hydroxyethylthio)acetamide | HCID 67725880 | — |
| 생성물 | N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-2-(2-butyryloxyethylthio)acetamide | HCID 67725830 | 88% |
반응 단계
Following a procedure similar to that described in Example 7, but using N-[4-(4-piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-2-(2-hydroxyethylthio)acetamide (prepared as described in Example 1) and butyryl chloride as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained in an 88% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05616579 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-6c8987d5d7ad4dd3b957641adaa52506 |
| 출처 메모 | uspto-grants-1997_04 |