Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonium Hydroxide → Thiophen-2-acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonium Hydroxide | HCID 14923 | — |
| 반응물 | 2-Thiopheneacetyl chloride | HCID 162362 | — |
| 생성물 | Thiophen-2-acetamide | HCID 78208 | 64% |
반응 단계
To a mixture of concentrated NH4OH (100 mL) and ice was added 2-thiopheneacetyl chloride (13.0 g, 80.9 mmol). The desired compound crystallized from the reaction mixture. Recrystallization from hot water gave 2-thiopheneacetamide (8.08 g, 64% yield) as white crystals. mp 146°-147° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05616596 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-d50cdad937b642df885f4e3877aa82ac |
| 출처 메모 | uspto-grants-1997_04 |