2-Propylhept-2-enal → 2-Propylheptanal

HRID 522251

반응식

HRID 522251 반응식
[CH2:1]([C:4](=[CH:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH:5]=[O:6])[CH2:2][CH3:3]>[Pd].[C]>[CH2:1]([CH:4]([CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH:5]=[O:6])[CH2:2][CH3:3]

참가 물질

3

반응물 1

HCID 1187452-Propylhept-2-enal

생성물 1

HCID 30186342-Propylheptanal수율 97.8%

시약·촉매·용매 1

HCID 178418390HCID 178418390, 화합물촉매

반응 조건

온도
75 °C

실험 절차

An autoclave was charged with 420 g of 2-propyl-2-heptenal and 4 g of a 5% Pd carbon powder (water content: 56%, manufactured by N.E. Chemcat Corporation), and the mixture was stirred at 75° C. for 1.5 hours under a hydrogen pressure of 1.5 MPa. The reaction product was filtered through a membrane filter (PTFE, 0.5 μm) to obtain 416 g of 2-propylheptanal.

후처리

  1. filtrationThe reaction product was filtered through a membrane
  2. filtrationfilter (PTFE, 0.5 μm)

출처 및 근거

ORD 기록
ord-f577967a37614483969cbe2e27e6788d
출처 데이터셋
uspto-grants-2016_05
특허 번호
US09328306B2

연결된 노트

불러오는 중…