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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 522337생성일: 2026년 10월 24일

4-Aminostyrene → 1-(4-Vinylphenyl)-3-[3,5-bis(trifluoromethyl)phenyl]thiourea

https://huagongshe.com/ko/reaction/522337

반응식

참여 물질

역할이름HCID투입량
반응물4-AminostyreneHCID 73700—
반응물3,5-Bis(trifluoromethyl)phenyl isothiocyanateHCID 2733395—
용매TetrahydrofuranHCID 8028—
생성물1-(4-Vinylphenyl)-3-[3,5-bis(trifluoromethyl)phenyl]thioureaHCID 5811244460%

반응 단계

To a stirred solution of 4-aminostyrene (3.5 mmol) in dry THF (20 mL) under nitrogen was added 3,5-bis-(trifluoromethyl)phenyl isothiocyanate (3.5 mmol). The solution was refluxed overnight and then the solvent was evaporated under reduced pressure. The resulting solid residue was purified by column chromatography to yield the desired product in 60% yield.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09329186B2
출처 데이터셋uspto-grants-2016_05
ORD IDord-3fe51d0a917048c28d43fc50b0e7264a
출처 메모uspto-grants-2016_05