참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Benzoyl Peroxide | HCID 7187 | — |
| 반응물 | 2-Ethylhexyl acrylate | HCID 7636 | — |
| 반응물 | Lauryl Methacrylate | HCID 8906 | — |
| 반응물 | 2-Ethylhexyl methacrylate | HCID 12713 | — |
| 용매 | Cyclohexane | HCID 8078 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | Dodecyl methacrylate 2-ethylhexyl methacrylate 2-ethylhexyl acrylate | HCID 86729957 | — |
반응 단계
An acrylic adhesive A was prepared in the following manner. A reaction liquid containing monomers including 13 parts by weight of dodecyl methacrylate, 78 parts by weight of 2-ethylhexyl methacrylate, and 9 parts by weight of 2-ethylhexyl acrylate, and 50 parts by weight of ethyl acetate was supplied to a 40-L polymerization apparatus. Subsequently, a nitrogen atmosphere at 80° C. was maintained in the polymerization apparatus. To the reaction liquid, a polymerization initiator solution prepared by dissolving 0.5 parts by weight of benzoyl peroxide in 50 parts by weight of cyclohexane was added over 24 hours to copolymerize the above monomers. After the completion of the polymerization, ethyl acetate was further added to the reaction liquid to obtain an acrylic adhesive solution A containing 35% by weight of the acrylic adhesive A including a dodecyl methacrylate/2-ethylhexyl methacrylate/2-ethylhexyl acrylate copolymer.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US09333182B2 |
|---|
| 출처 데이터셋 | uspto-grants-2016_05 |
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| ORD ID | ord-10134d1523fc427c880519c5679af08d |
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| 출처 메모 | uspto-grants-2016_05 |
|---|
