Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → S 20928
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Cyclobutanecarbonyl chloride | HCID 78705 | — |
| 반응물 | 2-(1-Naphthyl)ethylamine hydrochloride | HCID 12370437 | — |
| 용매 | Chloroform water | HCID 22418719 | — |
| 생성물 | S 20928 | HCID 127856 | — |
반응 단계
0.01 mol of N-[2-(1-naphthyl)ethyl]amine hydrochloride is dissolved in a water/chloroform (40: 60; vol/vol ) mixture, and 0.02 mol of potassium carbonate is then added with magnetic stirring. The reaction mixture is cooled in an ice bath, and 0.01 mol of cyclobutanecarbonyl chloride is then added dropwise with magnetic stirring.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05616614 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-8e4b4b7fd8854a2684e0c0c78407b175 |
| 출처 메모 | uspto-grants-1997_04 |