Potassium Carbonate → S 20928

HRID 52289

반응식

HRID 52289 반응식
Cl.[C:2]1([CH2:12][CH2:13][NH2:14])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1.C(=O)([O-])[O-].[K+].[K+].[CH:21]1([C:25](Cl)=[O:26])[CH2:24][CH2:23][CH2:22]1>O.C(Cl)(Cl)Cl>[C:2]1([CH2:12][CH2:13][NH:14][C:25]([CH:21]2[CH2:24][CH2:23][CH2:22]2)=[O:26])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 78705Cyclobutanecarbonyl chlorideHCID 123704372-(1-Naphthyl)ethylamine hydrochloride

생성물 1

HCID 127856S 20928

시약·촉매·용매 1

HCID 22418719Chloroform water용매

실험 절차

0.01 mol of N-[2-(1-naphthyl)ethyl]amine hydrochloride is dissolved in a water/chloroform (40: 60; vol/vol ) mixture, and 0.02 mol of potassium carbonate is then added with magnetic stirring. The reaction mixture is cooled in an ice bath, and 0.01 mol of cyclobutanecarbonyl chloride is then added dropwise with magnetic stirring.

후처리

  1. additionis then added with magnetic stirring
  2. temperatureThe reaction mixture is cooled in an ice bath

출처 및 근거

ORD 기록
ord-8e4b4b7fd8854a2684e0c0c78407b175
출처 데이터셋
uspto-grants-1997_04
특허 번호
US05616614

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