Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,8-Dichloroanthraquinone → 1,8-Bis{[2-(dimethylamino)ethyl]amino}anthracene-9,10-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,8-Dichloroanthraquinone | HCID 6708 | — |
| 반응물 | N,N-Dimethylethylenediamine | HCID 66053 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1,8-Bis{[2-(dimethylamino)ethyl]amino}anthracene-9,10-dione | HCID 14320119 | — |
반응 단계
A mixture of 1,8-dichloroanthraquinone (5.5 g, 20 mmol) and N,N-dimethylethylenediamine (40 mL) was refluxed for 18 h. The mixture was cooled to room temperature and diluted with water to precipitate the title compound which was recrystallised from methanol to afford Compound 6 (4.5 g). The structure of Compound 6 is given below:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09334281B2 |
| 출처 데이터셋 | uspto-grants-2016_05 |
| ORD ID | ord-0272c4eb373b4ee89275b9904cf25ac8 |
| 출처 메모 | uspto-grants-2016_05 |