3-(3-Ethoxy-4-nitrophenyl)-4-methyl-4H-1,2,4-triazole → 2-Ethoxy-4-(4-methyl-4H-1,2,4-triazol-3-yl)aniline

HRID 523089노트

반응식

HRID 523089 반응식
[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([C:13]2[N:17]([CH3:18])[CH:16]=[N:15][N:14]=2)[CH:7]=[CH:8][C:9]=1[N+:10]([O-])=O)[CH3:2]>CCOC(C)=O.CCO>[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([C:13]2[N:17]([CH3:18])[CH:16]=[N:15][N:14]=2)[CH:7]=[CH:8][C:9]=1[NH2:10])[CH3:2]

참가 물질

4

반응물 1

HCID 899956773-(3-Ethoxy-4-nitrophenyl)-4-methyl-4H-1,2,4-triazole

생성물 1

HCID 899956322-Ethoxy-4-(4-methyl-4H-1,2,4-triazol-3-yl)aniline

시약·촉매·용매 2

HCID 702Ethanol용매HCID 8857Ethyl Acetate용매

실험 절차

The title compound was prepared according to the method described for Preparation 107 using 3-(3-Ethoxy-4-nitrophenyl)-4-methyl-4H-1,2,4-triazole (Preparation 116) in EtOAc and EtOH (1:8 v:v).

출처 및 근거

ORD 기록
ord-f35e0841564844e4be4e1850f274898a
출처 데이터셋
uspto-grants-2016_05
특허 번호
US09334286B2

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