Ethyl 1-benzyl-4-methylpiperazine-2-carboxylate → Ethyl 4-methylpiperazine-2-carboxylate
반응식
C([N:8]1[CH2:13][CH2:12][N:11]([CH3:14])[CH2:10][CH:9]1[C:15]([O:17][CH2:18][CH3:19])=[O:16])C1C=CC=CC=1>[Pd]>[CH3:14][N:11]1[CH2:12][CH2:13][NH:8][CH:9]([C:15]([O:17][CH2:18][CH3:19])=[O:16])[CH2:10]1참가 물질
3
실험 절차
Ethyl 1-benzyl-4-methylpiperazine-2-carboxylate (11.54 g, 44 mmol) was reacted with Pd—C (10%, 1 g) according to the procedure as described in Example 34, Step C to give the title compound as colorless oil (6.2 g, 82%). The compound was characterized by the following spectroscopic data:
출처 및 근거
- ORD 기록
- ord-ec1f039cb0be49b58eca347e4a31fd6a
- 출처 데이터셋
- uspto-grants-2016_05
- 특허 번호
- US09340538B2
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