2-Amino-6-methoxybenzothiazole → 2-Cyano-6-methoxy benzothiazole

HRID 524800

반응식

HRID 524800 반응식
[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:6]2[N:7]=[C:8](N)[S:9][C:5]=2[CH:4]=1.[C:13]([Cu])#[N:14]>>[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:6]2[N:7]=[C:8]([C:13]#[N:14])[S:9][C:5]=2[CH:4]=1

참가 물질

3

실험 절차

6-methoxybenzo[d]thiazol-2-amine (9 g, 50 mmol) was reacted with CuCN (8.96 g, 100 mmol) according to the procedure as described in Example 61, Step A to give the title compound as a white solid (2.1 g, 22%). The compound was characterized by the following spectroscopic data:

출처 및 근거

ORD 기록
ord-f2c31f5651ce4d4bbb0f55cdedf1b63b
출처 데이터셋
uspto-grants-2016_05
특허 번호
US09340538B2

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