Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonium Chloride → 6-Methoxybenzo[d]thiazole-2-carboximidamide hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonium Chloride | HCID 25517 | — |
| 반응물 | 2-Cyano-6-methoxy benzothiazole | HCID 342109 | — |
| 반응물 | Sodium Methoxide | HCID 10942334 | — |
| 생성물 | 6-Methoxybenzo[d]thiazole-2-carboximidamide hydrochloride | HCID 118107613 | 75% |
반응 단계
6-methoxybenzo[d]thiazole-2-carbonitrile (1 g, 5.26 mmol) was reacted with sodium methoxide (0.28 g, 5.26 mmol) and ammonium chloride (0.6 g, 11 mmol) according to the procedure as described in Example 61, Step B to give the title compound as a white solid (0.96 g, 75%). The compound was characterized by the following spectroscopic data:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09340538B2 |
| 출처 데이터셋 | uspto-grants-2016_05 |
| ORD ID | ord-a5da7ede6b604060ad6e1da9b0089605 |
| 출처 메모 | uspto-grants-2016_05 |