Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → Civetone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Ethyl 17-oxocycloheptadec-8-ene-1-carboxylate | HCID 53673108 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Civetone | HCID 5315941 | — |
반응 단계
2-ethoxycarbonyl-9-cycloheptadecenone will be refluxed with about 10% NaOH in methanol for about 1 hour to give civetone. After completion of the reaction, the reaction mixture will be neutralized using about 10% sulfuric acid. The product will be extracted using ether and can be purified using silica-gel chromatography.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09346729B2 |
| 출처 데이터셋 | uspto-grants-2016_05 |
| ORD ID | ord-00fc4ff0450f49bc9168967cb6cbe090 |
| 출처 메모 | uspto-grants-2016_05 |