Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethoxysilane → Triethoxy(3-isocyanatopropyl)silane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethoxysilane | HCID 13830 | — |
| 반응물 | Allyl isocyanate | HCID 15123 | — |
| 용매 | P-Xylene | HCID 7809 | — |
| 생성물 | Triethoxy(3-isocyanatopropyl)silane | HCID 90613 | 71.8% |
반응 단계
In analogy to Example 6, a reaction mixture consisting of 640 g of p-xylene, 680 g (8.17 mol) of allyl isocyanate and 1250 g (7.6 mol) of triethoxysilane was reacted at from 76° to 92° C. over the course of 150 minutes. Working up by distillation gave 1350 g of 3-isocyanatopropyltriethoxysilane in addition to the trimer.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05616762 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-a6b7d28bd66448d9ab588797d7716d9f |
| 출처 메모 | uspto-grants-1997_04 |