Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Nitrobenzaldehyde → 2,6-Di-tert-butyl-4-[3-nitro-alpha-(piperidin-1-yl)benzyl]phenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Nitrobenzaldehyde | HCID 7449 | — |
| 반응물 | Piperidine | HCID 8082 | — |
| 반응물 | 2,6-Di-tert-butylphenol | HCID 31405 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | 2,6-Di-tert-butyl-4-[3-nitro-alpha-(piperidin-1-yl)benzyl]phenol | HCID 19963870 | 60% |
반응 단계
Using the same procedure described in Example 4, 30.2 g (0.2 mol) of 3-nitro-benzaldehyde, 37.4 g (0.44 mol) of piperidine and 39.2 g (0.19 mol) of 2,6-di-tert-butyl-phenol are allowed to react in xylene to give 48.4 g of the title compound as yellow crystals, melting at 157° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05616774 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-df448f9b88ca41edb7f97b5a94ee5ea8 |
| 출처 메모 | uspto-grants-1997_04 |