Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl (chloroformyl)acetate → Ethyl thiazole-5-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl (chloroformyl)acetate | HCID 118030 | — |
| 반응물 | Methanethioamide | HCID 3005587 | — |
| 생성물 | Ethyl thiazole-5-carboxylate | HCID 459108 | 33% |
반응 단계
According to the procedure of Mashraqui and Keehn (J. Am. Chem. Soc. 1982, 104, 4461), ethyl α-chloro-α-formylacetate was condensed with thioformamide and vacuum distilled to provide 5.65 g (33%) of the desired compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05616714 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-f3518c71ebc14df68b241e1171fe4697 |
| 출처 메모 | uspto-grants-1997_04 |