tert-Butyl Formate → HCID 68763133, 화합물

HRID 529072

반응식

HRID 529072 반응식
[CH2:1]([O:3][C:4](=[O:27])[CH2:5][C:6]1[CH:7]=[C:8]2[C:14]3([CH2:19][CH2:18][N:17](C(OCCCC)=O)[CH2:16][CH2:15]3)[CH:13]=[N:12][C:9]2=[CH:10][CH:11]=1)[CH3:2].[CH:28]([O:30][C:31]([CH3:34])([CH3:33])[CH3:32])=[O:29]>>[CH2:1]([O:3][C:4](=[O:27])[CH2:5][C:6]1[CH:7]=[C:8]2[C:14]3([CH2:19][CH2:18][N:17]([C:28]([O:30][C:31]([CH3:34])([CH3:33])[CH3:32])=[O:29])[CH2:16][CH2:15]3)[CH2:13][NH:12][C:9]2=[CH:10][CH:11]=1)[CH3:2]

참가 물질

3

반응물 2

HCID 61207tert-Butyl FormateHCID 69810198Butyl 5-(2-ethoxy-2-oxoethyl)spiro[indole-3,4'-piperidine]-1'-carboxylate

생성물 1

HCID 68763133HCID 68763133, 화합물

실험 절차

tert-butyl 5-(2-ethoxy-2-oxoethyl)spiro[indoline-3,4′-piperidine]-1′-carboxylate was prepared by the procedures described in Example 1, Step 2, substituting tert-butyl 5-chlorospiro[indole-3,4′-piperidine]-1′-carboxylate with butyl 5-(2-ethoxy-2-oxoethyl)spiro[indole-3,4′-piperidine]-1′-carboxylate. LCMS (APCI+) m/z 275.2 [M+H−Boc]+; Rt=3.58 min.

출처 및 근거

ORD 기록
ord-0f16b993c01745e283264e850836d300
출처 데이터셋
uspto-grants-2016_05
특허 번호
US09346805B2

연결된 노트

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