Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Boron Trichloride → Bnc-105
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Boron Trichloride | HCID 25135 | — |
| 반응물 | 2-Methyl-3-(3,4,5-trimethoxybenzoyl)-6-methoxy-7-isopropoxy-benzo[b]furan | HCID 60149020 | — |
| 생성물 | Bnc-105 | HCID 24786555 | 83% |
반응 단계
Note: A similar reaction when scaled-up with 2-methyl-3-(3,4,5-trimethoxybenzoyl)-6-methoxy-7-isopropoxy-benzo[b]furan (1.25 gm) and boron trichloride solution (1M solution in DCM, 3.1 mL) gave the title compound (930 mg, 83%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09346842B2 |
| 출처 데이터셋 | uspto-grants-2016_05 |
| ORD ID | ord-d13725b99129438ca02328f3c18d843d |
| 출처 메모 | uspto-grants-2016_05 |