HCID 19036218, 화합물 → HCID 178441659, 화합물

반응식

OC(C1N=C(CCC)NC=1C(OCC)=O)C.[C:17]([C:20]1[N:21]=[C:22]([CH2:30][CH2:31][CH2:32][CH3:33])[NH:23][C:24]=1[C:25]([O:27][CH2:28][CH3:29])=[O:26])(=[O:19])[CH3:18]>>[CH2:30]([C:22]1[NH:23][C:24]([C:25]([O:27][CH2:28][CH3:29])=[O:26])=[C:20]([CH:17]([OH:19])[CH3:18])[N:21]=1)[CH2:31][CH2:32][CH3:33]

참가 물질

반응물 2

HCID 19036218HCID 19036218, 화합물

HCID 178440097HCID 178440097, 화합물

생성물 1

HCID 178441659HCID 178441659, 화합물수율 85.2%

실험 절차

Following a procedure similar to that described in Preparation 23(iii), but using 0.64 g of ethyl 4-acetyl-2-butylimidazole-5-carboxylate [prepared as described in step (ii) above]. 0.55 g of the title compound was obtained as crystals, melting at 149° C.

출처 및 근거

ORD 기록: ord-887d8e329be54d08a2d86af58a720a59
출처 데이터셋: uspto-grants-1997_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05616599

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