Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4,4,5,5-Tetramethyl-2-(5-methylfuran-2-yl)-1,3,2-dioxaborolane → HCID 178486380, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4,4,5,5-Tetramethyl-2-(5-methylfuran-2-yl)-1,3,2-dioxaborolane | HCID 2736881 | — |
| 반응물 | 1-((3-Bromo-5-iodo-4-methoxyphenyl)diazenyl)pyrrolidine | HCID 66700101 | — |
| 생성물 | HCID 178486380 | HCID 178486380 | — |
반응 단계
1-((3-Bromo-5-iodo-4-methoxyphenyl)diazenyl)pyrrolidine (0.15 g, 0.366 mmol) and 4,4,5,5-tetramethyl-2-(5-methylfuran-2-yl)-1,3,2-dioxaborolane (0.076 g, 0.366 mmol), were reacted in the same manner as Example 1 Part B for 18 hours to give crude product which was purified on an Isco 12 g silica cartridge eluting with ethyl acetate/hexane (0% to 25%) to give the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09353091B2 |
| 출처 데이터셋 | uspto-grants-2016_05 |
| ORD ID | ord-f77667acca784a0b90667e81daeb8b1a |
| 출처 메모 | uspto-grants-2016_05 |