methyl 1-methyl-1H-pyrazole-3-carboxylate → 1-Methyl-1H-pyrazole-3-carboxamide

반응식

[CH3:1][N:2]1[CH:6]=[CH:5][C:4]([C:7]([O:9]C)=O)=[N:3]1.[NH3:11].O>>[CH3:1][N:2]1[CH:6]=[CH:5][C:4]([C:7]([NH2:11])=[O:9])=[N:3]1

참가 물질

반응물 2

HCID 7017175methyl 1-methyl-1H-pyrazole-3-carboxylate

HCID 12896473Azane;hydrate

생성물 1

HCID 134645861-Methyl-1H-pyrazole-3-carboxamide

실험 절차

A solution of methyl 1-methyl-1H-pyrazole-3-carboxylate (1.1 g, 7.9 mmol) in NH3.H2O (10 mL) was stirred for 2 h at room temperature. The solvent was evaporated to give the crude product which was used for the next step without further purification.

후처리

customThe solvent was evaporated

출처 및 근거

ORD 기록: ord-c756c510a23a4298a52158dbfa1c4385
출처 데이터셋: uspto-grants-2016_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09353104B2

반응 노트

불러오는 중…