참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-Bromodecane | HCID 8173 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 1H-1,2,4-Triazole, 3,5-dimethyl- | HCID 139001 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 1-Decyl-3,5-dimethyl-1,2,4-triazole | HCID 19047643 | — |
반응 단계
A mixture of 3,5-dimethyl-1,2,4-triazole (6.0 parts; 0.062 mol ex (b) above) and 1-bromodecane (14.4 parts; 0.065 mol) in dimethylformamide (16 ml) was heated together at 120° C. for 23 hours. The cooled reaction mixture was diluted with water (100 ml), a solution of sodium hydroxide (2.62 parts; 0.065 mol) in water (100 ml) added, and the product extracted into ether (3×50 ml). After drying over magnesium sulphate the solution was evaporated to yield a pale yellow oil (3.3 parts; 22% theory).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05620595 |
|---|
| 출처 데이터셋 | uspto-grants-1997_04 |
|---|
| ORD ID | ord-3009bdd309704dabb6eaebb5c0730e1c |
|---|
| 출처 메모 | uspto-grants-1997_04 |
|---|
