반응식
[CH2:1]([NH:8][CH:9]=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S-:11][C:12]#[N:13].[Na+:14]>>[CH2:1]([NH:8][CH:9]=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S-:11][C:12]#[N:13].[Na+:14]참가 물질
3
반응 조건
- 온도
- 30 °C
실험 절차
To a round-bottom flask, 9.9 g of purified N-benzyl formamide and 4 g of NaSCN (sodium thiocyanate) were introduced. The mixture was agitated gradually under nitrogen atmosphere at 30° C. for 40 minutes, and then at room temperature for 5 hours to obtain 10.7 g of N-benzyl formamide-NaSCN eutectic mixture.
출처 및 근거
- ORD 기록
- ord-92c554d1877b4115a46c924621464c74
- 출처 데이터셋
- uspto-grants-2014_10
- 특허 번호
- US08858837B2
연결된 노트
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