Thiomorpholine → 4-thiomorpholinophthalazin-1(2H)-one

HRID 535527노트

반응식

HRID 535527 반응식
Cl[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:5](=[O:12])[NH:4][N:3]=1.[NH:13]1[CH2:18][CH2:17][S:16][CH2:15][CH2:14]1>>[S:16]1[CH2:17][CH2:18][N:13]([C:2]2[C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5](=[O:12])[NH:4][N:3]=2)[CH2:14][CH2:15]1

참가 물질

3

반응물 2

HCID 67164ThiomorpholineHCID 27751424-chlorophthalazin-1(2H)-one

생성물 1

HCID 709757644-thiomorpholinophthalazin-1(2H)-one

실험 절차

4-chlorophthalazin-1(2H)-one and thiomorpholine were processed using a method similar to that described in Example 1A to afford the title compound. MS (APCI+) M/Z 248 (M+H)+.

출처 및 근거

ORD 기록
ord-754db3616564496d9f4ea4e10c74b662
출처 데이터셋
uspto-grants-2014_10
특허 번호
US08859549B2

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