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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 53565생성일: 2026년 10월 24일

Z-3-(1,3-dioxan-2-yl)-1-(2-pyridyl)-1-propene → 1-(1,3-Dioxan-2-yl)-3-(2-pyridyl)propane

https://huagongshe.com/ko/reaction/53565

반응식

참여 물질

역할이름HCID투입량
반응물Z-3-(1,3-dioxan-2-yl)-1-(2-pyridyl)-1-propeneHCID 70113689—
촉매PalladiumHCID 23938—
생성물1-(1,3-Dioxan-2-yl)-3-(2-pyridyl)propaneHCID 1969413992.5%

반응 단계

Through a suspension of 800 mg (4.2 mmol) of olefin 149 and 100 mg of 10% palladium on carbon was bubbled a steady stream of hydrogen gas for a period of 10 min. The reaction mixture was then filtered through celite and concentrated to give 805 mg of the acetal 150 as a colorless oil. 1H NMR consistent with structure.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05620971
출처 데이터셋uspto-grants-1997_04
ORD IDord-bf8ddce61e554c87a399e80c329d67fa
출처 메모uspto-grants-1997_04