Dimethylamine → 3-chloro-N,N-dimethylpropane-1-sulfonamide

HRID 536226노트

반응식

HRID 536226 반응식
[Cl:1][CH2:2][CH2:3][CH2:4][S:5](Cl)(=[O:7])=[O:6].[CH3:9][NH:10][CH3:11]>>[Cl:1][CH2:2][CH2:3][CH2:4][S:5]([N:10]([CH3:11])[CH3:9])(=[O:7])=[O:6]

참가 물질

3

반응물 2

HCID 674DimethylamineHCID 154103-Chloropropanesulphonyl chloride

생성물 1

HCID 100353283-chloro-N,N-dimethylpropane-1-sulfonamide

실험 절차

The procedure used for the preparation of Intermediate D was used to prepare the title compound from 3-chloropropanesulfonyl chloride and dimethylamine. High vacuum drying gave the title compound (2.1 g, 100%): 1H NMR (DMSO-d6) δ: 2.06-2.11 (2H, m), 2.75 (6H, s), 3.10-3.15 (2H, m), 3.72 (2H, t).

출처 및 근거

ORD 기록
ord-6752174e0ffa469aa497eeb1583e1dba
출처 데이터셋
uspto-grants-2014_10
특허 번호
US08859572B2

반응 노트

불러오는 중…