10-Undecyn-1-ol → 3-(9-Decynyloxy)benzenecarboxamide

반응식

[OH:1][C:2]1[CH:3]=[C:4]([C:8]([NH2:10])=[O:9])[CH:5]=[CH:6][CH:7]=1.[CH2:11](O)[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]#C>>[CH2:20]([O:1][C:2]1[CH:3]=[C:4]([C:8]([NH2:10])=[O:9])[CH:5]=[CH:6][CH:7]=1)[CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][C:12]#[CH:11]

참가 물질

반응물 2

HCID 7601510-Undecyn-1-ol

HCID 3424033-Hydroxybenzamide

생성물 1

HCID 594028653-(9-Decynyloxy)benzenecarboxamide

실험 절차

Synthesised from 3-hydroxybenzenecarboxamide and 10-undecyn-1-ol according to Method C, scheme 3; mp 111-112° C., HPLC-MS (method 1): m/z 274 [M+H]+, Rt=4.61 min.

출처 및 근거

ORD 기록: ord-bcd1e534ebca4a939d9f32902f56ebe1
출처 데이터셋: uspto-grants-2014_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08865736B2

반응 노트

불러오는 중…